Tetrahydrofuran → 4,4,5,5-Tetramethyl-2-(oxolan-3-yl)-1,3,2-dioxaborolane

HRID 1490407Notes

Reaction equation

HRID 1490407 reaction equation
C1CCOC1>CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.Cc1cc(C)c(-c2cnc3c(ccc4c(C[Si](C(C)C)(C(C)C)C(C)C)c(-c5c(C)cc(C)cc5C)cnc43)c2C[Si](C(C)C)(C(C)C)C(C)C)c(C)c1>CC1(C)OB(C2CCOC2)OC1(C)C

Participants

4

Reactant 1

HCID 8028Tetrahydrofuran

Product 1

HCID 111482974,4,5,5-Tetramethyl-2-(oxolan-3-yl)-1,3,2-dioxaborolaneYield 70%

Reagents, catalysts & solvents 2

HCID 2733548Bis(pinacolato)diboraneReagentHCID 178424575HCID 178424575, compoundReagent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-4e11887ae6914e2281edb2f5f34d49ce
Source dataset
Borylation dataset from Roche

Reaction notes

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