2-(4-methoxyphenyl)-1,3-benzoxazole → HCID 178488840, compound

HRID 1490449Notes

Reaction equation

HRID 1490449 reaction equation
COc1ccc(-c2nc3ccccc3o2)cc1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].Cc1cnc2c(ccc3c(C)c(C)cnc32)c1C.[Ir].[Ir]>COc1ccc(-c2nc3cccc(B4OC(C)(C)C(C)(C)O4)c3o2)cc1

Participants

6

Reactant 1

HCID 4838372-(4-methoxyphenyl)-1,3-benzoxazole

Product 1

HCID 178488840HCID 178488840, compoundYield 70%

Reagents, catalysts & solvents 4

HCID 742653,4,7,8-Tetramethyl-1,10-phenanthrolineReagentHCID 2733548Bis(pinacolato)diboraneReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-6386243d34d54e22aeaefd682a3c5e60
Source dataset
Borylation dataset from Roche

Reaction notes

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