M-Xylene → 2-(3,5-Dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1490645Notes

Reaction equation

HRID 1490645 reaction equation
Cc1cccc(C)c1>C1CCOC1.CC(C)[PH]1(C(C)C)Cc2cccc3[n]2->[Co]1([CH2][Si](C)(C)C)[PH](C(C)C)(C(C)C)C3.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C>Cc1cc(C)cc(B2OC(C)(C)C(C)(C)O2)c1

Participants

5

Reactant 1

HCID 7929M-Xylene

Product 1

HCID 159061982-(3,5-Dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneYield 11%

Reagents, catalysts & solvents 3

HCID 2733548Bis(pinacolato)diboraneReagentHCID 178460674HCID 178460674, compoundCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-4287abdd324f400681da3e5ae539b609
Source dataset
Borylation dataset from Roche

Reaction notes

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