3-Fluoro-N,N-dimethylbenzenesulfonamide → HCID 130058621, compound

HRID 1490649Notes

Reaction equation

HRID 1490649 reaction equation
CN(C)S(=O)(=O)c1cccc(F)c1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC(C)(C)c1ccnc(-c2cc(C(C)(C)C)ccn2)c1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir]>CN(C)S(=O)(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)c(F)c1

Participants

6

Reactant 1

HCID 606398363-Fluoro-N,N-dimethylbenzenesulfonamide

Product 1

HCID 130058621HCID 130058621, compoundYield 92%

Reagents, catalysts & solvents 4

HCID 2733548Bis(pinacolato)diboraneReagentHCID 42491874,4'-Di-tert-butyl-2,2'-bipyridylReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
50 °C

Sources & evidence

ORD record
ord-44fd82cea6b9447d81cb7574e978f24f
Source dataset
Borylation dataset from Roche

Reaction notes

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