N,N-diethyl-3-fluorobenzamide → HCID 139592774, compound

HRID 1490666Notes

Reaction equation

HRID 1490666 reaction equation
CCN(CC)C(=O)c1cccc(F)c1>C1=CCCC=CCC1.C1=CCCC=CCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CCN(C(C)C)C(C)C.C[OH2+].C[OH2+].[Ir].[Ir]>CCN(CC)C(=O)c1ccc(B2OC(C)(C)C(C)(C)O2)c(F)c1

Participants

5

Reactant 1

HCID 963334N,N-diethyl-3-fluorobenzamide

Product 1

HCID 139592774HCID 139592774, compoundYield 45%

Reagents, catalysts & solvents 3

HCID 2733548Bis(pinacolato)diboraneReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 81531DiisopropylethylamineSolvent

Conditions

Temperature
60 °C

Sources & evidence

ORD record
ord-c91951c814fe44fbae18d7cacbda49b2
Source dataset
Borylation dataset from Roche

Reaction notes

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