HCID 10944431, compound → HCID 178470587, compound

HRID 1490734Notes

Reaction equation

HRID 1490734 reaction equation
CCOC(=O)Cc1ccccc1C(=O)OCC>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC(C)(C)O.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].O=c1ccc2cccc(-c3ccc(-c4ccccn4)nc3)c2[nH]1.[Ir].[Ir].[K]>CCOC(=O)Cc1cc(B2OC(C)(C)C(C)(C)O2)ccc1C(=O)OCC

Participants

7

Reactant 1

HCID 10944431HCID 10944431, compound

Product 1

HCID 178470587HCID 178470587, compoundYield 63%

Reagents, catalysts & solvents 5

HCID 2733548Bis(pinacolato)diboraneReagentHCID 86639980Potassium tert-butoxideReagentHCID 1646813858-([2,2'-bipyridin]-5-yl)quinolin-2(1H)-oneReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
80 °C

Sources & evidence

ORD record
ord-74a71764ab9a46e58a956ef26ccdbaa9
Source dataset
Borylation dataset from Roche

Reaction notes

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