Menthol → HCID 178438912, compound

HRID 1490996Notes

Reaction equation

HRID 1490996 reaction equation
CC1CCC(C(C)C)C(O)C1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCCCCCC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.CC1(C)OBOC1(C)C.C[OH2+].C[OH2+].Cc1ccc2ccc3cccnc3c2n1.[Ir].[Ir]>CC(C)C1CCC(CB2OC(C)(C)C(C)(C)O2)CC1O

Participants

7

Reactant 1

HCID 1254Menthol

Product 1

HCID 178438912HCID 178438912, compoundYield 49%

Reagents, catalysts & solvents 5

HCID 2733548Bis(pinacolato)diboraneReagentHCID 27347684,4,5,5-Tetramethyl[1,3,2]dioxaborolaneReagentHCID 49133562-Methyl-1,10-phenanthrolineReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 9266CyclooctaneSolvent

Conditions

Temperature
100 °C

Sources & evidence

ORD record
ord-2abe2a2916f140dba3e92b0810f3cb28
Source dataset
Borylation dataset from Roche

Reaction notes

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