N-(1-naphthyl)hexanamide → HCID 178445135, compound

HRID 1491031Notes

Reaction equation

HRID 1491031 reaction equation
CCCCCC(=O)Nc1cccc2ccccc12>C1=CCCC=CCC1.C1=CCCC=CCC1.CC(C)[Si](Oc1ccc2ccccc2c1-c1c(Op2oc3ccc4ccccc4c3c3c(ccc4ccccc43)o2)ccc2ccccc12)(C(C)C)C(C)C.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.COC1CCCC1.C[OH2+].C[OH2+].Cc1cccc(C)n1.Cc1ccccc1.O=C(Nc1ccccc1-c1cccnc1)NC1CCCCC1.[Ir].[Ir]>CCC(CCC(=O)Nc1cccc2ccccc12)B1OC(C)(C)C(C)(C)O1

Participants

9

Reactant 1

HCID 532117N-(1-naphthyl)hexanamide

Product 1

HCID 178445135HCID 178445135, compoundYield 85%

Reagents, catalysts & solvents 7

HCID 79372,6-LutidineReagentHCID 2733548Bis(pinacolato)diboraneReagentHCID 154720182(11bR)-4-[[(1R)-2'-[[Tris(1-methylethyl)silyl]oxy][1,1'-binaphthalen]-2-yl]oxy]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepinReagentHCID 1559360261-Cyclohexyl-3-(2-pyridin-3-ylphenyl)ureaReagentHCID 76001521Bis(1,5-cyclooctadiene)dimethoxydiiridiumCatalystHCID 1140TolueneSolventHCID 138539Cyclopentyl methyl etherSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-e6a4bd7389284df0905548787c57849d
Source dataset
Borylation dataset from Roche

Reaction notes

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