3-Bromotoluene → 2-(3-Bromo-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

HRID 1491270Notes

Reaction equation

HRID 1491270 reaction equation
Cc1cccc(Br)c1>C1CCOC1.C1CCc2c(c3c(c4c2CCCC4)CCCC3)C1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.Cc1cnc2c(ccc3c(C)c(C)cnc32)c1C>Cc1cc(Br)cc(B2OC(C)(C)C(C)(C)O2)c1

Participants

6

Reactant 1

HCID 115603-Bromotoluene

Product 1

HCID 534290562-(3-Bromo-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneYield 0%

Reagents, catalysts & solvents 4

HCID 742653,4,7,8-Tetramethyl-1,10-phenanthrolineReagentHCID 95278DodecahydrotriphenyleneReagentHCID 2733548Bis(pinacolato)diboraneReagentHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-e40fa307b0874722bc9da9d218e704e6
Source dataset
Borylation dataset from Roche

Reaction notes

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