Ethyl Bromide → N-(2-Ethoxyphenyl)-N'-(1-octyloxy-2,2,6,6-tetramethylpiperidin-4-yl)oxamide
Reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]([C:11]([NH:13][CH:14]1[CH2:19][C:18]([CH3:21])([CH3:20])[N:17]([O:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])[C:16]([CH3:32])([CH3:31])[CH2:15]1)=[O:12])=[O:10].C(=O)([O-])[O-].[K+].[K+].[CH2:39](Br)[CH3:40]>>[CH2:39]([O:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9]([C:11]([NH:13][CH:14]1[CH2:15][C:16]([CH3:31])([CH3:32])[N:17]([O:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])[C:18]([CH3:20])([CH3:21])[CH2:19]1)=[O:12])=[O:10])[CH3:40]Participants
4
Procedure
The above-named compound is prepared by reacting the compound prepared in Example 13A with potassium carbonate and ethyl bromide.
Workup
- customThe above-named compound is prepared
Sources & evidence
- ORD record
- ord-4c38f9576f034cdbadc92c6606056cac
- Source dataset
- uspto-grants-1991_06
- Patent number
- US05021478
Reaction notes
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