1,2-Dichloroethane → HCID 12414417, compound

HRID 1494721Notes

Reaction equation

HRID 1494721 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[CH3:8].Cl[CH2:10][CH2:11]Cl>>[CH3:1][C:2]1[C:7]([CH3:8])=[C:6]([CH2:8][CH2:7][C:6]2[CH:5]=[CH:4][CH:3]=[C:2]([CH3:1])[C:10]=2[CH3:11])[CH:5]=[CH:4][CH:3]=1

Participants

3

Procedure

o-Xylene and 1,2-dichloroethane were reacted in the presence of anhydrous AlC13 catalyst to obtain 1,2-di(dimethylphenyl)ethane (bromine number: 0.1) of 136 to 148° C. in distillation temperature at 3 to 5 mmHg. This was cracked in the like manner as in Example 1.

Sources & evidence

ORD record
ord-9ae955193ef54b59a9157b8c94a46b1b
Source dataset
uspto-grants-1991_06
Patent number
US05026939

Reaction notes

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