Hydrogen Bromide → HCID 11791475, compound

HRID 1502612Notes

Reaction equation

HRID 1502612 reaction equation
Br.[NH2:2][C@H:3]([C:14]([OH:16])=[O:15])[CH2:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][CH:6]=1.N1([C:29](=O)[C:28]2N(C)C=N[C:23]=2N(C)C1=O)C.C1(C)CCC(C(C)C)C(O)C1>O>[CH:28]([O:15][C:14](=[O:16])[C@H:3]([CH2:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[NH:7][CH:6]=1)[NH2:2])([CH3:29])[CH3:23]

Participants

6

Reactant 4

HCID 260Hydrogen BromideHCID 1254MentholHCID 2519CaffeineHCID 6305L-Tryptophan

Product 1

HCID 11791475HCID 11791475, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

HBr (120 g) and tryptophan (5 g) were dissolved in water (1 L). Caffeine (100 g) and menthol (10 g) were added into the mixture and the mixture was stirred for a few minutes. The mixture was filled into either spray bottles or roll-on bottles.

Workup

  1. additionThe mixture was filled into either spray bottles or roll-on bottles

Sources & evidence

ORD record
ord-016f479544dd4ddf8a541d9c6e3c5937
Source dataset
uspto-grants-2015_12
Patent number
US09211249B2

Reaction notes

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