Hydrochloric Acid → HCID 178447682, compound

HRID 1504252Notes

Reaction equation

HRID 1504252 reaction equation
[Cl-:1].[Cl-].[Cl-].[O:4]=[V+3:5].[CH2:6]([OH:11])[C:7]([CH3:10])([CH3:9])[CH3:8].Cl>C1(C)C=CC=CC=1>[Cl-:1].[CH2:6]([O:11][V+:5]([O:11][CH2:6][C:7]([CH3:10])([CH3:9])[CH3:8])=[O:4])[C:7]([CH3:10])([CH3:9])[CH3:8]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 6404Neopentyl alcoholHCID 178478621HCID 178478621, compound

Product 1

HCID 178447682HCID 178447682, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Added to a glass bottle with a capacity of 200 ml sealed with a rubber stopper after drying and nitrogen substitution were 0.05 mol of VOCl3 (oxovanadium trichloride), 0.10 mol of neopentyl alcohol, and toluene. Then, hydrochloric acid generated while bubbling with nitrogen was removed through a needle to obtain a toluene solution of dineopentoxy oxovanadium chloride.

Workup

  1. additionAdded to a glass bottle with a capacity of 200 ml
  2. customsealed with a rubber stopper
  3. customafter drying
  4. customwhile bubbling with nitrogen
  5. customwas removed through a needle

Sources & evidence

ORD record
ord-387169aa93e244aabe9d96e844684b87
Source dataset
uspto-grants-2015_12
Patent number
US09212274B2

Reaction notes

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