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With stirring and ice cooling, 111 g of triethylamine was added to a mixture of 120 g of methacrylic acid chloride, 170 g of 1-hydroxyacenaphthene, and 1500 g of toluene. The mixture was stirred at room temperature for 16 hours. By standard aqueous work-up and solvent distillation, a crude product was obtained. It was purified by column chromatography, yielding the target compound, acenaphthenyl methacrylate.

1. stirringThe mixture was stirred at room temperature for 16 hours
2. distillationBy standard aqueous work-up and solvent distillation
3. customa crude product was obtained
4. customIt was purified by column chromatography