2-Iodophenol → HCID 58488457, compound

HRID 1510085Notes

Reaction equation

HRID 1510085 reaction equation
[I:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].C(=O)([O-])[O-].[K+].[K+].[CH3:15][O:16][CH2:17][CH2:18]Br>C(#N)C>[I:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[O:8][CH2:18][CH2:17][O:16][CH3:15]

Participants

5

Reactant 3

HCID 107842-IodophenolHCID 11430Potassium CarbonateHCID 809722-Bromoethyl methyl ether

Product 1

HCID 58488457HCID 58488457, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

To a mixture of 2-iodophenol (5.00 g, 22.7 mmol) and potassium carbonate (4.71 g, 34.1 mmol) in ACN (7 ml) was added 2-bromoethyl methyl ether (3.79 g, 27.3 mmol).

Sources & evidence

ORD record
ord-f06b5c9b57d54653b79209799905a85a
Source dataset
uspto-grants-2012_07
Patent number
US08211885B2

Reaction notes

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