HRID1515031

反应详情

EQUATION

反应方程式

HRID 1515031 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 4-amino-N-(4-tert-butylphenyl)-3-nitrobenzamide from the previous step and 100 mg of 5% platinum on carbon in 50 mL of 1:1 ethyl acetate/ethanol was reduced under a hydrogen balloon. The reaction was filtered through Celite to remove catalyst and the solvent was removed under reduced pressure to afford 3,4-diamino-N-(4-tert-butylphenyl)-benzamide.

WORKUP

后处理

  1. filtrationThe reaction was filtered through Celite
  2. customto remove catalyst
  3. customthe solvent was removed under reduced pressure