HRID1527693

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCOC(=O)/C(C)=C/c1c(SC)c(OC)c2ccccc2c1OC

HCID46180104

未命名化合物

$结构：COc1cc(/C=C(\C)C(=O)O)c(OC)c2ccccc12$

HCID46180242

未命名化合物

PRODUCTS

生成物

$结构：COc1c(/C=C(\C)C(=O)O)c(SC)c(OC)c2ccccc12$

HCID46180316

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Compound 99h was prepared from 98h (0.165 g, 0.476 mmol) as described above for 29a to give 0.181 g (0.568 mmol, 118%) of the product as a orange solid following flash chromatography (1:3 EtOAc:hexanes 0.5% AcOH) and recrystallization from Et2O/hexanes.

WORKUP

后处理

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