2,6-Dibromopyridine → 2-Bromo-6-phenylpyridine

HRID 1529126Notes

Reaction equation

HRID 1529126 reaction equation
Br[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Br:8])[N:3]=1.[C:9]1(B(O)O)[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[Br:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:3]=1

Participants

3

Reactant 2

HCID 122742,6-DibromopyridineHCID 66827Phenylboronic Acid

Product 1

HCID 5686792-Bromo-6-phenylpyridine

Procedure

Prepared according to the procedure described in Example 3, Step 5, using 2,6-dibromo-pyridine and phenylboronic acid. After purification the product still contained some 2,6-dibromo-pyridine starting material. The mixture was used directly in the next step.

Workup

  1. customPrepared
  2. customAfter purification the product

Sources & evidence

ORD record
ord-6e4e35316296437fbd690a7e543cfdbf
Source dataset
uspto-grants-2015_07
Patent number
US09090573B2

Reaction notes

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