反应详情

温度

120 °C

p-Cyclohexylphenol (83.1 g (0.5 mol)) was dissolved in 300 ml of toluene, and 150 g of 2-chloroethyl vinyl ether was added thereto. Furthermore, 25 g of sodium hydroxide, 5 g of tetrabutylammonium bromide and 60 g of triethylamine were added, and the resulting mixture was heated with stirring at 120° C. for 5 hours. The reaction solution was washed with water, and excess chloroethyl vinyl ether and toluene were removed by distillation under reduced pressure. From the obtained oil, the objective p-cyclohexylphenoxyethyl vinyl ether (X-1) was obtained by distillation under reduced pressure.

1. temperaturethe resulting mixture was heated
2. washThe reaction solution was washed with water, and excess chloroethyl vinyl ether and toluene
3. customwere removed by distillation under reduced pressure