HRID1532091

反应详情

EQUATION

反应方程式

HRID 1532091 的结构方程式

PROCEDURE

实验过程

In a similar manner to Example 49 reaction of 2-(2-propoxyphenyl)purin-6-one (0.81 g) with chlorosulphonic acid (4.5 ml), followed by reaction with methylamine in industrial methylated spirit (33%, 50 ml) yielded the title compound, 0.49 g, m.p. 245-246° C. (recrystallised twice from aqueous ethanol).