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HRID1534440

反应详情

EQUATION

反应方程式

HRID 1534440 的结构方程式

REACTANTS

反应物

2
结构：O=C(C1NCCCC1O)N1CCCC1
HCID15165787

未命名化合物

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：OC1CCCNC1CN1CCCC1
HCID15123236

2-(1-Pyrrolidinylmethyl)-3-piperidinol

C10H20N2O

收率 65.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

By reducing 5 g (0.025 moles) of 2-(pyrrolidin-1-yl)carbonyl-3-hydroxy piperidine, with 1.2 g (0.025 moles) of LiAlH4 in 100 ml of dry THF, using an alkaline work-up, 3 g of the title compound were obtained.