Dichloromethane → (2,3-Dihydrobenzo[b][1,4]dioxin-2-yl)methyl 4-methylbenzenesulfonate

HRID 1554851Notes

Reaction equation

HRID 1554851 reaction equation
[CH3:13][CH2:14][N:15]([CH2:16][CH3:17])[CH2:18][CH3:19].[Cl:31][CH2:32][Cl:33].[O:1]1[CH:2]([CH2:11][OH:12])[CH2:3][O:4][c:5]2[c:6]1[cH:7][cH:8][cH:9][cH:10]2.[c:20]1([CH3:30])[cH:21][cH:22][c:23]([S:26](=[O:27])(=[O:28])[Cl:29])[cH:24][cH:25]1>>[O:1]1[CH:2]([CH2:11][O:12][S:26]([c:23]2[cH:22][cH:21][c:20]([CH3:30])[cH:25][cH:24]2)(=[O:27])=[O:28])[CH2:3][O:4][c:5]2[c:6]1[cH:7][cH:8][cH:9][cH:10]2

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 73974-Toluenesulfonyl chlorideHCID 8471TriethylamineHCID 193141,4-Benzodioxane-2-methanol

Product 1

HCID 4522296(2,3-Dihydrobenzo[b][1,4]dioxin-2-yl)methyl 4-methylbenzenesulfonate

Sources & evidence

ORD record
ord-95ebe047f5b44198915701b99ef589dd
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (1/10)

Reaction notes

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