HRID15573

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CC=CCN(c1ccc2c(c1)nc(CCC)n2CC(=O)OC(C)(C)C)S(=O)(=O)c1ccc(F)cc1

HCID67200276

未命名化合物

PRODUCTS

生成物

结构：CC=CCN(c1ccc2c(c1)nc(CCC)n2CC(=O)O)S(=O)(=O)c1ccc(F)cc1

HCID67200878

未命名化合物

PROCEDURE

实验过程

{5-[But-2-enyl-(4-fluoro-benzenesulfonyl)-amino]-2-propyl-benzoimidazol-1-yl}-acetic acid tert-butyl ester was treated with TFA (2 mL) for 2 hours, concentrated, and purified by preparative LCMS to give the title compound. MS calculated for C22H24FN3O4S—H: 444, observed: 444.

WORKUP

后处理

concentrationconcentrated
custompurified by preparative LCMS