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HRID1576324

反应详情

EQUATION

反应方程式

HRID 1576324 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CC(=O)OCC
HCID7761

Diethyl propanedioate

C7H12O4

结构：CN(C(N)=O)c1ccccc1
HCID78316

1-METHYL-1-PHENYL UREA

C8H10N2O

结构：C[O-].[Na+]
HCID10942334

Methanol, sodium salt

CH3NaO

PRODUCTS

生成物

1
结构：CN1C(=O)CC(=O)N(c2ccccc2)C1=O
HCID15545494

1-Methyl-3-phenylpyrimidine-2,4,6(1H,3H,5H)-trione

C11H10N2O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

1-Phenyl-3-methyl-barbituric acid was prepared by condensation of malonic acid diethyl ester with phenyl-methylurea in methanol, with addition of sodium methylate. It melts at about 124°C after recrystallization from toluene.

WORKUP

后处理

  1. customIt melts at about 124°C after recrystallization from toluene