4-Aminobenzoic Acid → HCID 16228385, compound

HRID 1576700Notes

Reaction equation

HRID 1576700 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[CH:11]1([C:14](Cl)=[O:15])[CH2:13][CH2:12]1.[CH2:17](N(CC)CC)[CH3:18]>>[CH:11]1([C:14]([NH:1][C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=2)=[O:15])[CH2:13][CH2:12][CH2:18][CH2:17]1

Participants

4

Reactant 3

HCID 9784-Aminobenzoic AcidHCID 8471TriethylamineHCID 77637Cyclopropanecarbonyl chloride

Product 1

HCID 16228385HCID 16228385, compound

Procedure

4-Cyclopentanecarbonylamino-benzoic acid was prepared as described in Example 1B from 31.5 g (0.23 mol) of p-aminobenzoic acid and 17.3 g (0.23 mol) of cyclopropanecarboxylic acid chloride in the presence of triethylamine.

Sources & evidence

ORD record
ord-9594126feedd456bb8160c82ed60d6c3
Source dataset
uspto-grants-1976_09
Patent number
US03982011

Reaction notes

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