HRID1578471

反应详情

EQUATION

反应方程式

HRID 1578471 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

An aqueous emulsion comprising 45 parts by weight of methylmethacrylate, 7 parts by weight of styrene, 48 parts by weight of n-butylacrylate, and containing 0.18 part by weight of 30 percent hydrogen peroxide and 0.95 part by weight of C14 -fatty amine hydrochloride dissolved therein, is added dropwise at 85°C. over a period of 4 - 6 hours to an aqueous solution comprising 0.05 part by weight of C14 -fatty amine hydrochloride, 0.005 part by weight of iron (II) chloride, and 0.02 part by weight of 30 percent hydrogen peroxide. The dispersion obtained is subsequently combined with 4 parts by weight of an adduct formed between isononyl phenol and 100 mols of ethylene oxide. A coagulate-free dispersion having a solids content of about 50 percent is obtained.

WORKUP

后处理

  1. dissolutiondissolved
  2. additionis added dropwise at 85°C. over a period of 4 - 6 hours to an aqueous solution
  3. customThe dispersion obtained