Chlorotrimethylsilane → HCID 12472499, compound

HRID 1580660Notes

Reaction equation

HRID 1580660 reaction equation
[NH:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6].[CH3:7][Si:8]([CH3:11])([CH3:10])Cl.C(N(CC)CC)C>O1CCCC1>[CH3:7][Si:8]([CH3:11])([CH3:10])[N:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6]

Participants

5

Reactant 3

HCID 6397ChlorotrimethylsilaneHCID 8471TriethylamineHCID 2723650Ethylenethiourea

Product 1

HCID 12472499HCID 12472499, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried in a vacuum desiccator.

Workup

  1. filtrationThe warm suspension was freed of the precipitated triethylamine hydrochloride by filtration
  2. customthe filtrate was evaporated
  3. customdried in a vacuum desiccator

Sources & evidence

ORD record
ord-0aa091b00ff444f69ed0591853196c06
Source dataset
uspto-grants-1976_01
Patent number
US03933795

Reaction notes

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