HRID1583559

反应详情

EQUATION

反应方程式

HRID 1583559 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 150 g (1.23 mole) of 4-hydroxybenzaldehyde and 30 g (0.52 mole) of acetone in 600 ml of absolute ethanol was cooled while passing in hydrogen chloride for 45 minutes. After two hours of stirring, ice water was added and the resulting dark solid was filtered off. It was crystallized from absolute ethanol to give 90 g of brown, crystalline product.

WORKUP

后处理

  1. filtrationthe resulting dark solid was filtered off
  2. customIt was crystallized from absolute ethanol
  3. customto give 90 g of brown, crystalline product