Hydrochloric Acid → HCID 13430196, compound

HRID 1583743Notes

Reaction equation

HRID 1583743 reaction equation
C(OC([NH:8][CH2:9][C:10]([NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:19]1[O:24][C:23](=[O:25])[C:22]2[CH:26]=[CH:27][CH:28]=[CH:29][C:21]=2[N:20]=1)=[O:11])=O)(C)(C)C.[ClH:30]>C(OCC)(=O)C>[ClH:30].[NH2:8][CH2:9][C:10]([NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:19]1[O:24][C:23](=[O:25])[C:22]2[CH:26]=[CH:27][CH:28]=[CH:29][C:21]=2[N:20]=1)=[O:11]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 20258244HCID 20258244, compound

Product 1

HCID 13430196HCID 13430196, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

2-[2-(tert-butyloxycarbonyl)aminoethanoyl]aminophenyl-3,1-benzoxazin-4-one (45 mg) was reacted in ethyl acetate with hydrogen chloride under reaction conditions as described for the synthesis of compounds of Example 9, Method A, to afford the above-titled compound.

Sources & evidence

ORD record
ord-39ef339885d542b9adac530082649cd0
Source dataset
uspto-grants-1985_11
Patent number
US04554272

Reaction notes

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