Hydrochloric Acid → HCID 131717974, compound

HRID 1587589Notes

Reaction equation

HRID 1587589 reaction equation
CC(C)(OC([NH:7][C@H:8]([C:13]([NH:15][CH:16]([CH2:25][CH:26]1[CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1)[CH:17]([P:19]([O:23][CH3:24])([O:21][CH3:22])=[O:20])[OH:18])=[O:14])[CH2:9][CH:10]([CH3:12])[CH3:11])=O)C.[ClH:33]>C(OCC)(=O)C>[ClH:33].[CH:26]1([CH2:25][C@H:16]([NH:15][C:13](=[O:14])[C@H:8]([CH2:9][CH:10]([CH3:11])[CH3:12])[NH2:7])[CH:17]([P:19]([O:23][CH3:24])([O:21][CH3:22])=[O:20])[OH:18])[CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 86746934HCID 86746934, compound

Product 1

HCID 131717974HCID 131717974, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The title compound of Example 1 (2.29 g, 4.8 mmol) was dissolved in a 1.2N solution of hydrochloric acid in ethyl acetate (25 mL). After 1 hour, the reaction mixture was concentrated yielding 2.2 g of the title A compound.

Workup

  1. concentrationthe reaction mixture was concentrated
  2. customyielding 2.2 g of the title A compound

Sources & evidence

ORD record
ord-f0782f004d69450fa0cdfb1145e6fb5a
Source dataset
uspto-grants-1993_06
Patent number
US05217958

Reaction notes

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