huagongshe.com
HRID1590973

反应详情

EQUATION

反应方程式

HRID 1590973 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：O=C(OCc1ccccc1)[C@@H]1CCCN1
HCID736155

未命名化合物

结构：C[C@@H](OCc1ccccc1)[C@H](NC(=O)OC(C)(C)C)C(=O)O
HCID1549483

N-[(1,1-Dimethylethoxy)carbonyl]-O-(phenylmethyl)-L-threonine

C16H23NO5

PRODUCTS

生成物

1
结构：C[C@@H](OCc1ccccc1)[C@H](NC(=O)OC(C)(C)C)C(=O)N1CCC[C@H]1C(=O)OCc1ccccc1
HCID15003996

未命名化合物

收率 95.3%

PROCEDURE

实验过程

By using 8.66 g of Boc-Thr(Bzl)-OH and 7.42 g of HCl.H-Pro-OBzl, and the same procedure as in Reference Example 15 was repeated to obtain 13.25 g (yield: 95.3%) of the above mentioned objective product.

WORKUP

后处理

  1. customto obtain 13.25 g (yield: 95.3%) of the