反应详情

The product from step e (0.79 g, 6.4 mmol) was dissolved in 100 mL of MeOH and added carefully to 0.20 g of 10% Pd/C under N2. The mixture was hydrogenated in a Parr shaker at 50 PSI overnight. Filtration through fiberglass filter paper under N2 and under vacuum yielded 0.56 g of a clear colorless oil.

1. customwas hydrogenated in a Parr shaker at 50 PSI overnight
2. filtrationFiltration through fiberglass
3. filtrationfilter paper under N2