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HRID1592523

反应详情

EQUATION

反应方程式

HRID 1592523 的结构方程式

REACTANTS

反应物

3
结构：Cc1cccnc1C=O
HCID1501874

3-methylpyridine-2-carbaldehyde

C7H7NO

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：CC(NCCCNC(=O)OC(C)(C)C)c1ccccn1
HCID67272175

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccnc1CN(CCCNC(=O)OC(C)(C)C)C(C)c1ccccn1
HCID67273022

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of [3-(1-pyridin-2-yl-ethylamino)-propyl]-carbamic acid tert-butyl ester and 3-methyl-pyridine-2-carboxaldehyde with NaBH(OAc)3 in CH2Cl2 gave {3-[(3-methyl-pyridin-2-ylmethyl)-(1-pyridin-2-yl-ethyl)-amino]-propyl}-carbamic acid tert-butyl ester as a colorless oil.