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HRID1592663

反应详情

EQUATION

反应方程式

HRID 1592663 的结构方程式

REACTANTS

反应物

3
结构：CC(N)c1ccccn1
HCID541877

1-(2-Pyridinyl)ethanamine

C7H10N2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：C[Si](C)(C)CCOCn1c(C=O)nc2ccccc21
HCID12017128

未命名化合物

PRODUCTS

生成物

1
结构：CC(NCc1nc2ccccc2n1COCC[Si](C)(C)C)c1ccccn1
HCID67272285

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of 1-(2-trimethylsilanyl-ethoxymethyl)-1H-benzimidazole-2-carbaldehyde in CH2Cl2 with 1-pyridin-2-yl-ethylamine and NaBH(OAc)3 gave (1-pyridin-2-yl-ethyl)-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-benzimidazol-2-ylmethyl]-amine as a pale green oil.