Piperazine → HCID 58996620, compound

HRID 1592711Notes

Reaction equation

HRID 1592711 reaction equation
[NH:1]1[CH2:6][CH2:5][NH:4][CH2:3][CH2:2]1.Br[C:8]1[C:13]([N+:14]([O-:16])=[O:15])=[CH:12][CH:11]=[CH:10][C:9]=1[CH3:17]>>[CH3:17][C:9]1[CH:10]=[CH:11][CH:12]=[C:13]([N+:14]([O-:16])=[O:15])[C:8]=1[N:1]1[CH2:6][CH2:5][NH:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 4837PiperazineHCID 2318282-Bromo-3-nitrotoluene

Product 1

HCID 58996620HCID 58996620, compound

Procedure

1-(2-Methyl-6-nitrophenyl]piperazine was prepared in a manner similar to Preparation 1A except that piperazine was coupled to 2-bromo-1-methyl-3-nitro-benzene. LRMS (ESI+): 222.4 (M+1)

Sources & evidence

ORD record
ord-d180201cf01847c58e5a93ab389ef4c5
Source dataset
uspto-grants-2007_11
Patent number
US07291619B2

Reaction notes

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