Water → Prop-2-enamide;styrene

HRID 1596106Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1596106
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.C(C1C=CC=CC=1C=C)=C.O>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Komponenten

6

Edukt 4

HCID 962WaterHCID 6579AcrylamideHCID 7501StyreneHCID 666661,2-Diethenylbenzene

Produkt 1

HCID 168235Prop-2-enamide;styrene

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Polystyrenesulfonate (15.0 mmoles, 2.612 g), acrylamide (7.2 mmoles, 0.512 g), styrene (7.2 mmoles, 0.8250 mL) and divinylbenzene (0.6 mmoles, 85.5 microL) were dissolved in 10 mL ethanol and 10 mL water in a 40 mL vial fitted with a septa cap. The solution was degassed by bubbling nitrogen through and 1 mole % AIBN was added as a solution. The polymerization solution was further degassed and the placed in a heated reaction block at 60° C. for 18 h. A clear, colorless gel formed.

Aufarbeitung

  1. customThe solution was degassed
  2. customby bubbling nitrogen through and 1 mole % AIBN
  3. additionwas added as a solution
  4. customThe polymerization solution was further degassed
  5. customthe placed in a heated reaction block at 60° C. for 18 h
  6. customA clear, colorless gel formed

Quellen und Nachweise

ORD-Eintrag
ord-38bdcf3d312741beafc610e0ab25132f
Quelldatensatz
uspto-grants-2001_09
Patentnummer
US06290946B1

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