Phenol → HCID 15546411, compound

HRID 1600955Notes

Reaction equation

HRID 1600955 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].[Na+].[O:10]1[CH2:12][CH:11]1[CH2:13][CH2:14][C:15]1[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=1>CN(C)C=O>[O:7]([CH2:12][CH:11]([OH:10])[CH2:13][CH2:14][C:15]1[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=1)[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

5

Reactant 3

HCID 996PhenolHCID 24758Sodium hydrideHCID 10877288HCID 10877288, compound

Product 1

HCID 15546411HCID 15546411, compoundYield 16.4%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared according to the method described in Example 1a) from phenol (0.15 g), sodium hydride (0.075 g) and 3-(2-oxiranylethyl)pyridine (0.15 g) in dimethylformamide at 100° C. for 30 minutes to give the title compound as an oil (0.04 g).

Workup

  1. customPrepared
  2. customat 100° C.
  3. customfor 30 minutes

Sources & evidence

ORD record
ord-b42bfa79773943b6aaf6c321cbf4946e
Source dataset
uspto-grants-1999_11
Patent number
US05977105

Reaction notes

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