Ammonium Hydroxide → HCID 18779060, compound

HRID 1601740Notes

Reaction equation

HRID 1601740 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][O:10][CH2:11][C:12]([OH:14])=O.C(Cl)(=O)C(Cl)=O.[OH-].[NH4+:22]>C1(C)C=CC=CC=1>[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][O:10][CH2:11][C:12]([NH2:22])=[O:14]

Participants

5

Reactant 3

HCID 14923Ammonium HydroxideHCID 65578Oxalyl chlorideHCID 187790542-[2-(2-Methylphenyl)ethoxy]acetic acid

Product 1

HCID 18779060HCID 18779060, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The subtitle compound (5.02 g) was prepared according to the procedure in example 5 part b using 2-[2-(2-methylphenyl)ethoxy]acetic acid (6.726 g), oxalyl chloride (6.22 ml), concentrated ammonium hydroxide (60 ml), and toluene (60 ml).

Sources & evidence

ORD record
ord-25f22b8712ef49159ad4d493eb1e9679
Source dataset
uspto-grants-1999_11
Patent number
US05977384

Reaction notes

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