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HRID1601923

反应详情

EQUATION

反应方程式

HRID 1601923 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Cc1ccc(S(=O)(=O)O)cc1.O=C(NC1(Cc2ccccc2)CCNCC1)N1CCCC1
HCID21200488

未命名化合物

结构：CN(C)C(=O)NC1(c2ccccc2)CCN(CCC2(c3ccc(F)c(F)c3)CN(C(=O)c3ccccc3)CCO2)CC1.CN(C)C(=O)NC1(c2ccccc2)CCN(CCC2(c3ccc(F)c(F)c3)CN(C(=O)c3ccccc3)CCO2)CC1.Cl.Cl.O
HCID131720058

未命名化合物

PRODUCTS

生成物

1
结构：Cl.O=C(NC1(Cc2ccccc2)CCN(CCC2(c3ccc(F)c(F)c3)CN(C(=O)c3ccccc3)CCO2)CC1)N1CCCC1
HCID21200480

未命名化合物

收率 131.8%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

This compound is prepared by the procedure described in EXAMPLE 45 from 1.2 g of the compound obtained in step C of EXAMPLE 37, 1.5 g of 4-benzyl-4-(pyrrolidin-1-ylcarbonylamino)piperidine p-toluenesulfonate, 1.2 g of K2CO3 and 3 ml of DMF to give 0.83 g of the expected product. M.p.=140° C.

WORKUP

后处理

  1. customThis compound is prepared by the procedure