Ethanol → HCID 11148304, compound

HRID 1604267Notes

Reaction equation

HRID 1604267 reaction equation
[CH2:1]([OH:3])[CH3:2].[C:4]([O:10][CH2:11][CH3:12])(=[O:9])[CH2:5][C:6]([CH3:8])=[O:7].[C:13](OCC)(=O)[CH3:14]>>[CH3:13][CH:14]1[CH:5]([C:4]([O:10][CH2:11][CH3:12])=[O:9])[C:6](=[O:7])[CH2:8][C:1](=[O:3])[CH2:2]1

Participants

4

Reactant 3

HCID 702EthanolHCID 8857Ethyl AcetateHCID 8868Ethyl Acetoacetate

Product 1

HCID 11148304HCID 11148304, compound

Procedure

The same procedure used above is modified using an equivalent amount of anhydrous ethanol as the solvent and ethyl acetoacetate; yield 93.4 g (47%); mp 89-91° C. (from ethyl acetate: petroleum ether, bp 54° C.).

Sources & evidence

ORD record
ord-a4510bfc15504edab76df5488755a213
Source dataset
uspto-grants-1999_11
Patent number
US05994349

Reaction notes

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