HRID1615747

反应详情

EQUATION

反应方程式

HRID 1615747 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.50 g (2.0 mmol) 5-amino-1,3-dihydrospiro[inden-2,3′-pyrrolo[2,3-b]pyridin]-2′(1′H)-one in 20 ml DCM were combined with 0.27 g (2 mmol) N-chlorosuccinimide versetzt and stirred for 5 h at RT. The mixture was evaporated down and the residue was purified by HPLC.

WORKUP

后处理

  1. customThe mixture was evaporated down
  2. customthe residue was purified by HPLC