HRID1617123

反应详情

EQUATION

反应方程式

HRID 1617123 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product from step (iv) (3.8 g) was dissolved in DCM (100 mL) and TFA (35 mL) and the reaction mixture stirred at rt for 16 h. The solvent was evaporated and the residue taken up in MeOH. The product was purified via SCX resin to give the subtitle compound 2.3 g.

WORKUP

后处理

  1. customThe solvent was evaporated
  2. customThe product was purified via SCX resin