HRID1620734

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID21866389

未命名化合物

$结构：O=C(CNC1=NC(=O)S/C1=C\C1CCN(Cc2ccc(C(F)(F)F)cc2C(F)(F)F)CC1)NC1CC1$

HCID178521294

未命名化合物

PRODUCTS

生成物

$结构：Cl.O=C(CNC1=NC(=O)S/C1=C\C1CCN(Cc2ccc(C(F)(F)F)cc2C(F)(F)F)CC1)NC1CC1$

HCID178479699

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

To a solution of N2-[(5Z)-5-({1-[2,4-bis(trifluoromethyl)benzyl]piperidin-4-yl}methylidene)-2-oxo-2,5-dihydro-1,3-thiazol-4-yl]-N-cyclopropylglycinamide (700 mg) in THF (10 mL) was added a solution of 4N hydrogen chloride/ethyl acetate (0.33 mL), and the precipitate was so collected by filtration to give the title compound (301 mg).

WORKUP

后处理

filtrationthe precipitate was so collected by filtration