Hydrochloric Acid → HCID 131713884, compound

HRID 1632431Notes

Reaction equation

HRID 1632431 reaction equation
[NH:1](C(OCC1C=CC=CC=1)=O)[C@H:2]([C:7]([NH:9][C@H:10]([C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH2:11][CH:12]([CH3:14])[CH3:13])=[O:8])[CH2:3][C:4](=[O:6])[NH2:5].[ClH:30]>CO.[Pd]>[NH2:1][C@H:2]([C:7]([NH:9][C@H:10]([C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH2:11][CH:12]([CH3:14])[CH3:13])=[O:8])[CH2:3][C:4](=[O:6])[NH2:5].[ClH:30]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 131713883HCID 131713883, compound

Product 1

HCID 131713884HCID 131713884, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

3.01 Grams of Z-Asn-Leu-OEt was dissolved in 50 ml of methanol and 7.4 ml of 1N-HCl, the solution was subjected to catalytical reduction in the presence of 500 mg of palladium black at a room temperature, under an atmospheric pressure to obtain H-Asn-Leu-OEt.HCl.

Sources & evidence

ORD record
ord-a3217a0c92d748e7b2e8a520d35de1a4
Source dataset
uspto-grants-1984_10
Patent number
US04474754

Reaction notes

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