1-Nitropropane → HCID 54235658, compound

HRID 1633110Notes

Reaction equation

HRID 1633110 reaction equation
[C:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)([O:3][CH3:4])=[O:2].[N+:13]([CH2:16][CH2:17][CH3:18])([O-:15])=[O:14]>>[C:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=[C:16]([N+:13]([O-:15])=[O:14])[CH2:17][CH3:18])=[CH:7][CH:6]=1)([O:3][CH3:4])=[O:2]

Participants

3

Reactant 2

HCID 79031-NitropropaneHCID 15294Methyl 4-Formylbenzoate

Product 1

HCID 54235658HCID 54235658, compound

Procedure

The title compound was prepared in an identical manner to that described in Description 27 using 4-carbomethoxybenzaldehyde and 1-nitropropane. τ(d6DMSO) 8.8 (3H, t, J=7 Hz), 8.08 (3H, s), 7.19 (2H, q, J=7 Hz), 6.12 (3H, s), 2.38 (2H, d, J=8 Hz), 1.97 (2H, d, J=8 Hz), 1.97 (1H, s).

Sources & evidence

ORD record
ord-73fbe20598d24c50ae97dedc333cc24b
Source dataset
uspto-grants-1984_10
Patent number
US04478849

Reaction notes

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