HRID1637687

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6395

Methanesulfonic acid

CH4O3S

结构：CCC(CC)Oc1cc(C)nc(Oc2c(C)cc(C)cc2C)c1C

HCID9818802

CP-316311

C21H29NO2

PRODUCTS

生成物

结构：CCC(CC)Oc1cc(C)[nH+]c(Oc2c(C)cc(C)cc2C)c1C.CS(=O)(=O)[O-]

HCID18800624

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

2 次

PROCEDURE

实验过程

4-(1-ethyl-propoxy)-3,6-dimethyl-2-(2,4,6-trimethyl-phenoxy)-pyridine (prepared as described in Example 1) was treated with 1 equivalent of methanesulfonic acid in ethyl acetate. The white crystals formed from ethyl acetate, melting point 117-119° C.