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HRID1637949

反应详情

EQUATION

反应方程式

HRID 1637949 的结构方程式

REACTANTS

反应物

4
结构：O
HCID962

Water

H2O

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：CCOC(=C1C(=O)N(C(C)=O)c2ccc([N+](=O)[O-])cc21)c1ccccc1
HCID54280104

未命名化合物

结构：Nc1ccc(Cc2c[nH]cn2)cc1
HCID178507529

未命名化合物

PRODUCTS

生成物

1
结构：O=C1Nc2ccc([N+](=O)[O-])cc2/C1=C(/Nc1ccc(Cc2c[nH]cn2)cc1)c1ccccc1
HCID178517251

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Prepared by reacting 1-acetyl-3-{1-ethoxy-1-phenylmethylidene}-5-nitro-2-indolinone with 1.45 equivalents of 4-(4-amino-benzyl)-1H-imidazole in DMF (100° C., for 2 hours), subsequent treatment with 5 equivalents of piperidine (20° C., 1 hour) and precipitation with water.

WORKUP

后处理

  1. customPrepared