HRID1639367

反应详情

EQUATION

反应方程式

HRID 1639367 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

70.0 g of 8-chloro-3,4-dihydro-2(1H)-naphthalenone are boiled at reflux for 2.5 hours in 550 ml of benzene and 33 ml of pyrrolidine in the presence of 1.4 g of p-toluenesulfonic acid. The crude 1-(8-chloro-3,4-dihydro-2-naphthyl)-pyrrolidine obtained is processed without purification.