HRID1640115

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6871

Diethyl ethoxymethylenemalonate

C10H16O5

HCID7732

4-Methoxybenzenamine

C7H9NO

PRODUCTS

生成物

HCID618981

Diethyl [(4-methoxyanilino)methylidene]propanedioate

C15H19NO5

PROCEDURE

实验过程

A mixture of 4methoxyaniline (28.3 g, 0.230 mol) in diethyl ethoxymethylene-malonate (46.0 mL, 0.230 mol) was allowed to stir at rt for 16 h. Removal of solvent gave diethyl ([(4-methoxyphenyl)aniino]methylenelmalonate. LCMS: (FA) ES+ 294.2.

WORKUP

后处理

customRemoval of solvent
customgave diethyl ([(4-methoxyphenyl)aniino]methylenelmalonate