反应详情

4-[(5,6-Dimethoxy-1-indanon-2-ylidene)methyl]pyridine (2.5 g) was dissolved in methylene chloride (60 ml) and chilled. m-Chloroperbenzoic acid (2.0 g) was added to reaction mixture and then stirred for 4 hours. Solid obtained was filtered. The wet solid so obtained was stirred with 10% sodium bicarbonate solution. The solid was filtered, washed with acetone and then dried to get the title compound (2.5 g).

1. temperaturechilled
2. customSolid obtained
3. filtrationwas filtered
4. customThe wet solid so obtained
5. filtrationThe solid was filtered
6. washwashed with acetone
7. customdried